Simple Italian Microscope (circa 1686)


Galleria
License Info
Image Use
Custom Photos
Partners
Site Info
Contact Us
Publications
Home

The Galleries:

Photo Gallery
Silicon Zoo
Pharmaceuticals
Chip Shots
Phytochemicals
DNA Gallery
Microscapes
Vitamins
Amino Acids
Birthstones
Religion Collection
Pesticides
BeerShots
Cocktail Collection
Screen Savers
Win Wallpaper
Mac Wallpaper
Movie Gallery
 

Spike (M.I.) Walker

Diaminodiphenylmethane/Sulphur Complex

English photomicrographer Spike (M.I.) Walker has been a consistent winner of the Nikon Small World competition for many years and has published many articles and a book about microscopy. Featured below is a photomicrograph of a diaminodiphenylmethane mixture with sulphur.

Diaminodiphenylmethane/sulphur complex

The two materials (diaminodiphenylmethane and sulphur) were mixed together on a microscope slide and melted under a cover glass. As soon as melting of all the constituents was complete, the cover glass was pressed down in order to reduce the thickness of the preparation and the slide quickly removed from the hotplate (an inverted electric iron is a good substitute). The specimen was photographed under crossed polarized illumination. The objective was a plan apochromat 10x/0.32 NA coupled to an achromatic condenser. The microscope was a Zeiss Ultraphot III equipped with an automatic 35-millimeter photohead. The film was Fujichrome Velvia. (10x)

Diaminodiphenylmethane, commonly referred to as dianilinemethane, is a weak nitrogen base having two analine moieties coupled to a methylene group at the para aromatic position. The chemical is highly toxic and crystallizes in light brown crystallites that slowly oxidize in air to form a darker oxidation product.

Sulphur is a nonmetallic chemical element belonging to the oxygen family (Group VIa of the periodic table) and is one of the most reactive of the elements. Pure sulfur is a tasteless, odorless, brittle solid that is pale yellow in color, a poor conductor of electricity, and insoluble in water. It was known to the ancients and referred to as brimstone in the Old Testament. Sulphur was first classified as an element in 1777 by Antoine Lavoisier and is estimated to be the ninth most abundant element in the universe. It makes up about 0.03 percent of the Earth's crust and is the most abundant constituent of minerals.

Free sulphur occurs primarily in volcanic or sedimentary deposits throughout the world, with heavy concentrations located in the sediments of the Gulf coast of North America. Sulphur compounds can be found in coal, petroleum, and natural gas and in sulfide ores such as pyrite (iron disulfide), galena (lead sulfide), cinnabar (mercury sulfide), sphalerite (zinc sulfide), and chalcopyrite (copper iron sulfide), as well as sulfates such as gypsum (calcium sulfate) and barite or heavy spar (barium sulfate).

BACK TO SPIKE WALKER GALLERY

Questions or comments? Send us an email.
Text and graphics for this article are
© 2000-2022 by Spike (M. I.) Walker.
All Rights Reserved under copyright law.
© 1995-2022 by Michael W. Davidson and The Florida State University. All Rights Reserved. No images, graphics, software, scripts, or applets may be reproduced or used in any manner without permission from the copyright holders. Use of this website means you agree to all of the Legal Terms and Conditions set forth by the owners.
This website is maintained by our
Graphics & Web Programming Team
in collaboration with Optical Microscopy at the
National High Magnetic Field Laboratory.
Last modification: Friday, Nov 13, 2015 at 02:18 PM
Access Count Since November 18, 2000: 11624
Microscopes provided by:
Visit the Nikon website. Visit the Olympus Microscopy Resource Center website.